technifyed

IIT Madras via NPTEL

Material Characterization

Overview

Metallurgy and Material Science course by Prof.S. Sankaran.

Syllabus 12

  1. How does an NPTEL online course work?
    • Properties of light, Image formation
    • Magnification and resolution
    • Depth of field,focus and field of view
  2. week-02
    • Lens defects,filters and light microscopy introduction
    • Optical microscope demo., Bright field imaging, opaque specimen illumination
    • Opaque stop microscopy, Phase contrast microscopy
    • Dark field microscopy, Polarization microscopy
  3. week-03
    • Differential interference contrast and fluorescence microscopy
    • Sample preparation techniques for optical microscopy
    • Tutorial problems
    • continuation-Tutorial problems
  4. week-04
    • Introduction to scanning electron Microscopy
    • Lens aberrations, Object resolution, Image quality
    • Interaction between electrons and sample, Imaging capabilities
    • SEM and its mode of operation, Effect of aperture size,Working distance,condenser lens strength
  5. week-05
    • SEM and its mode of operation- continuation
    • Factors affecting Interaction volume, Demonstration of SEM
    • Image formation and interpretation
    • Image formation and interpretation continued, EDS, WDS
  6. week-06
    • Special contrast mechanisms, Monte Carlo simulations of Interaction volume
    • Electron channeling contrast imaging (ECCI), (EBSD)-Theory & instrument demonstration
    • Tutorial Problems on SEM
  7. week-07
    • Basics of X-ray emission from source, electron excitation and X-ray interaction
    • Properties of X-rays
    • Bragg's Law Derivation
    • Diffraction relationship with reciprocal space
  8. week-08
    • X-ray scattering
    • Factors affecting intensities of X-ray peaks
    • Factors affecting intensities of X-ray peaks- continuation
    • Effect of crystallite size and strain on intensity of X-rays
  9. week-09
    • Profile fit, Factors affecting peak brodening
    • Indexing of diffraction pattern, Quantitative analysis
    • Indexing, Quantitative analysis-continuation, Residual stress measurements
    • XRD and Residual stress measurement- lab demonstration
  10. week-10
    • XRD Tutorial - 1
    • XSD Tutorial -2
    • Introduction to Transmission Electron Microscopy (TEM)
    • Fundementals of Transmission Electron Microscopy (TEM)
  11. week-11
    • Basics of Diffraction-1
    • Basics of Diffraction-2
    • TEM imaging-1
    • TEM imaging-2
  12. week-12
    • TEM instrument demonstration
    • TEM sample preparation-1-
    • TEM sample preparation-2
    • TEM Tutorial - 1
    • TEM Tutorial - 2

Advantages and disadvantages

Advantages

  • Taught by IIT and IISc professors, and it follows the Indian university syllabus closely.
  • All videos and assignments are free on NPTEL and SWAYAM.
  • The certificate is recognised by many Indian universities for credit transfer and by GATE aspirants.
  • Great for GATE and semester exam preparation.
  • Taught by Indian Institute of Technology Madras, one of the strongest names in its field.
  • Completely free.
  • Self-paced: start any time.
  • A clear syllabus (12 parts) you can see before you start.

Disadvantages

  • The certificate needs a proctored exam at a centre, which has a fee.
  • Recorded classroom lectures: thorough, but slower than made-for-online courses.
  • New runs start on fixed dates (January and July).
  • Learning is free, but the certificate costs money.

Some points apply to every course of this kind; see how we rank.

Free to learn

  • Free: Every video and assignment is free on NPTEL and SWAYAM. Enrol when the next run opens.
  • Certificate: Optional. It needs a proctored exam at a centre, which has a fee.

Taught by

  • Prof.S. SankaranIIT Madras

Indian Institute of Technology Madras is in Tier 1: world-leading universities and India's top institutes of our institution ranking (96/100). Runs NPTEL and the online BS in Data Science.

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